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iRubric: Spectroscopy LAB REPORT rubric

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Spectroscopy LAB REPORT FORMAL LAB REPORT Chemistry spectroscopy lab rubric Rubric Code: B24A8A4 By kalindim Ready to use Public Rubric Subject: Chemistry Type: (Other) Grade Levels: Undergraduate

Completeness and Quality of Data 50 % Completeness and Quality of Data as requested in guidelines and class
	Outstanding 10 pts	Good 8 pts	Satisfactory 4 pts	Poor 0 pts
IR Data Worth up to 2 points	Outstanding Attached, All KEY Peaks Picked, Printed as it should be Relevant bonds of functional groups written on the IR Spectra as show in class.	Good Attached, Some Key Peaks Picked, Printed as it should be Some Relevant bonds of functional groups written on the IR Spectra as show in class.	Satisfactory Attached, no peaks picked, something wrong with printing No relevant bonds of Fn groups written on IR spectra	Poor Not attached, or wrong compounds
Proton Data	Outstanding Attached, All Peaks Picked, Integration are completed, Integrations calibrated appropriately . Proton spectra is calibrated. The intensity of the peaks are appropriate	Good Attached, Some Peaks Picked, Integration are maybe be only partially completed, Integrations may not be calibrated appropriately . Proton spectra is calibrated. The intensity of the peaks might be too big or too small.	Satisfactory Attached, No Peaks Picked, No integrations or wrongly done Proton spectra not calibrated. The intensity of the peaks are not appropriate	Poor Not attached or done wrongly
Carbon-13 Data	Outstanding Attached, All Peaks Picked, Carbon spectra is calibrated. The intensity of the peaks are appropriate	Good Attached, NOT All Peaks Picked, Carbon spectra is may or may not be calibrated. The intensity of the peaks are not appropriate	Satisfactory Attached, NO Peaks Picked, Carbon spectra not be calibrated. The intensity of the peaks are not appropriate	Poor Not attached.
2D Data : HSQC and HMBC	Outstanding Attached. The intensity of the correlations are appropriate. Proper 1D spectra are on F2 and F1 axis 2D date is marked up in such a way to indicate that spectra have been used in the solution. Ie - proton and carbons are written on the 1D sides.	Good Attached. The intensity of the correlations are not appropriate OR Proper 1D spectra are not on F2 and F1 axis 2D date is marked up in such a way to indicate that spectra have been used in the solution. Ie - proton and carbons are written on the 1D sides.	Satisfactory Attached. The intensity of the correlations are not appropriate OR Proper 1D spectra are not on F2 and F1 axis 2D date is NOT marked up in such a way to indicate that spectra have been used in the solution. Ie - proton and carbons are written on the 1D sides.	Poor Not attached.
2D Data: COSY and DEPT 135	Outstanding Attached. The intensity of the correlations are appropriate. Proper 1D spectra are on F2 and F1 axis For DEPT135 -peaks are picked 2D date is marked up in such a way to indicate that spectra have been used in the solution. Ie - proton and carbons are written on the 1D sides.	Good Attached. For DEPT135 -peaks are picked The intensity of the correlations are not appropriate OR Proper 1D spectra are not on F2 and F1 axis 2D date is marked up in such a way to indicate that spectra have been used in the solution. Ie - proton and carbons are written on the 1D sides.	Satisfactory Attached. For DEPT135 -peaks are NOT picked The intensity of the correlations are not appropriate OR Proper 1D spectra are not on F2 and F1 axis 2D date is marked up in such a way to indicate that spectra have been used in the solution. Ie - proton and carbons are written on the 1D sides.	Poor Not attached.
Completeness of Report 30 % Completeness of Report as requested in the above guidelines: 30%
	Outstanding 6 pts	Good 4 pts	Satisfactory 2 pts	Poor 0 pts
Structure with appropriate numbering	Outstanding Structure with appropriate numbering	Good 1 to 2 things wrong with numbernig	Satisfactory 3 to 4 things wrong with numbernig	Poor More than 4 things wrong with numbernig
Table	Outstanding Table with appropriate numbering and chemical shifts entered correctly; right J values, and appropriate correlations	Good 2 to 4 things wrong with Table list in Outstanding	Satisfactory 5 to 8 things wrong with Table list in Outstanding	Poor More than 8 things wrong with Table list in Outstanding
Paragraph of description	Outstanding All elements in sample paragraph addressed, including data used, IR, mass etc. Clear description of what data points led to the assignment of the structure. Flow relatively logical. Chemical formatting correct as shown in paragraph	Good 2 to 4 things wrong with Table list in Paragraph of description	Satisfactory 5 to 8 things wrong with Table list in Paragraph of description	Poor More than 8 things wrong with Table list in Paragraph of description
List of Data points and References	Outstanding List of Data points done correctly and match attached data References included and right format	Good 2 to 3 things wrong with List of Data points and References	Satisfactory 4 to 6 things wrong with List of Data points and References	Poor More than 6 things wrong with List of Data points AND NO References
Identification of Compound and Correct Assignment 20 %
	Outstanding 4 pts	Good 3 pts	Satisfactory 2 pts	Poor 1 pts
Identification of Compound	Outstanding Id All Correct	Good 1 thing wrong (could be 2 things swapped)	Satisfactory 2 things wrong (could be 4 things swapped exactly)	Poor More than 2 things wrong
Correct Assignment of Chemical Shifts	Outstanding All Chemical Shifts assignment correct	Good .2 to 3 assignments wrong	Satisfactory 4 to 6 assignments wrong	Poor More than 6 assignments wrong

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